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- 详细信息
- 文献和实验
- 技术资料
- 英文名:
2-(((Tert-Butyldimethylsilyl)Oxy)Methyl)-7-Iodofuro3,2-CPyridine
- 库存:
999
- 供应商:
智溯科ZSK
- CAS号:
1956364-46-7
- 规格:
10mg/100mg/1184mg
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文献和实验RNA Synthesis Using 2-O-(Tert-Butyldimethylsilyl) Protection
This chapter enables the reader to carry out the solid-phase synthesis of ribonucleic acid (RNA) using β-cyanoethyl phosphoramidite chemistry combined with tert -butyldimethylsilyl protection of the ribose 2′-hydroxyl group. Phosphoramidite
are extracted by mixed-mode solid phase extraction. The benzodiazepine extracts are derivatized with N-methyl-N-(tert-butyldimethylsilyl)trifluoroacetamide (MTBSFTA) producing tert-butyldimethyl silyl derivatives; the alprazolam extracts are reconstituted
. GC-MS methods based on the conversion into tert -butyldimethylsilyl (33 ) and N(O,S)-propoxycarbonyl propyl ester (34 ) derivatives, and LC-MS method were highly sensitive and specific, but these methods require expensive equipment. Furthermore, CZE
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