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- Merck
- 美国
- 8.41873.0025
- 2026年02月12日
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文献和实验Synthesis of 2-O-Alkyloligoribonucleotides
7 ), ethyl (8 ), allyl (9 ), or butyl (10 ), with most studies being carried out with the methyl and allyl analogs.
2‐Bromoethanol (12 ; Sigma‐Aldrich, cat. no. B65586) (2‐bromoethoxy)(tert ‐butyl)dimethylsilane, 99% pure (13 ; Sigma‐Aldrich, cat. no. 428426)
Solid-Phase Synthesis of Neuropeptides by Fmoc Strategies
, and the side-chain protecting groups are removed by treating the peptide-resin with a mixture of trifluoroacetic acid and various ion scavengers (3 ). Methyl t-butyl ether is then added to precipitate the peptide out of the cleavage mixture. The crude
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