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tert-Butyl(2-(4-((tert-butyldimethylsilyl)oxy)-7a-methyloctahydro-1H-inden-1-yl)propoxy)dimethylsilane
N/A
C₂₅H₅₂O₂Si₂
440.85
Colourless viscous syrup
Chloroform
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文献和实验tert-Butyl(2-(4-((tert-butyldimethylsilyl)oxy)-7a-methyloctahydro-1H-inden-1-yl)propoxy)dimethylsilane
N/A
C₂₅H₅₂O₂Si₂
440.85
Colourless viscous syrup
Chloroform
. GC-MS methods based on the conversion into tert -butyldimethylsilyl (33 ) and N(O,S)-propoxycarbonyl propyl ester (34 ) derivatives, and LC-MS method were highly sensitive and specific, but these methods require expensive equipment. Furthermore, CZE
Figure 14.9.1 Synthesis of the propargylated dinucleoside phosphate triester 5 . Abbreviations: DMTr, 4,4′‐dimethoxytrityl; Lev, levulinyl; TBDMS, tert ‐butyldimethylsilyl; GiBu , 2‐( N ‐isobutyryl)guanin‐9‐yl. Adapted with permission
Synthesis of Peptidomimetic Conjugates of Cyclic Nucleoside Phosphonates
to 200 mesh, 1% cross‐linked, typical loading 1.0 to 1.8 mmol/g; Aldrich) Methyl O‐[tert‐butyl(dimethyl)silyl]‐(L )‐serinate ( S.6 a , see protocol
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