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- CAS号：
27784-76-5
tert-Butyl 2-(diethylphosphono)acetate
27784-76-5
C₁₀H₂₁O₅P
252.24
Colourless Oil
Chloroform (Slightly), Ethyl Acetate (Slightly)
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文献和实验tert-Butyl 2-(diethylphosphono)acetate
27784-76-5
C₁₀H₂₁O₅P
252.24
Colourless Oil
Chloroform (Slightly), Ethyl Acetate (Slightly)
Synthesis of Building Blocks and Oligonucleotides with {G}O6‐Alkyl‐O6{G} Cross‐Links
Introduction Basic Protocol 1: Protection of the Diol with a tert‐Butyldiphenyl Silyl Group Basic Protocol 2: Synthesis of O6‐2′‐Deoxyguanosine‐Alkyl‐O6‐2′‐Deoxyguanosine‐3′‐O‐bis‐Phosphoramidites
2‐Bromoethanol (12 ; Sigma‐Aldrich, cat. no. B65586) (2‐bromoethoxy)(tert ‐butyl)dimethylsilane, 99% pure (13 ; Sigma‐Aldrich, cat. no. 428426)
, without mercuric chloride? [ B-5 is: Water 90 ml Formalin (40% HCHO) 10 ml Mercuric chloride 6 g Sodium acetate (anhydrous) 1.25 g The sodium acetate brings the pH into the 5.8-6.0 range. Fix by immersion, 12-24 hours, then transfer to 70-80% alcohol
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